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真空燒結爐是怎樣工作的
發布時間:2022-08-07   瀏覽:1560次

  真(zhen)空燒結爐(lu)是(shi)怎樣工作的(de)

  真空燒結爐是一種用于制(zhi)備高性能(neng)陶瓷(ci)、金屬和合金材(cai)料的設備,它通過在真空(kong)或保(bao)護氣氛下將材(cai)料加熱(re)來實現。其工(gong)作(zuo)原理如(ru)下:

  1.加載樣品(pin):將需要制備的(de)(de)材料(liao)放置在燒結爐(lu)的(de)(de)樣品(pin)托盤(pan)上,然后將其放入(ru)燒結爐(lu)中(zhong)封好爐(lu)門。

真空燒結爐

  2.抽真(zhen)空(kong)(kong):打開燒(shao)結爐(lu)的(de)(de)抽真(zhen)空(kong)(kong)系統(tong),將(jiang)爐(lu)內(nei)氣體(ti)抽出(chu)(chu)并(bing)降至(zhi)所需的(de)(de)真(zhen)空(kong)(kong)度(du)。通(tong)常,在(zai)抽真(zhen)空(kong)(kong)時(shi)要先(xian)使用機械泵將(jiang)大部分的(de)(de)空(kong)(kong)氣和氣體(ti)抽出(chu)(chu)。當(dang)真(zhen)空(kong)(kong)度(du)降至(zhi)一定水平時(shi),就可(ke)以啟動效率高(gao)的(de)(de)擴散泵或分子泵,以進一步降低(di)真(zhen)空(kong)(kong)度(du)。這些泵可(ke)以更有效地抽出(chu)(chu)氣體(ti)分子,在(zai)實現更高(gao)真(zhen)空(kong)(kong)度(du)的(de)(de)同(tong)時(shi)提供更快的(de)(de)抽速。

  3.加熱(re):開(kai)始加熱(re)燒結(jie)(jie)爐,以達(da)到所需(xu)的(de)溫(wen)度。通常,燒結(jie)(jie)需(xu)要在高(gao)溫(wen)下進行,以使樣(yang)品達(da)到足夠的(de)致密度。

  4.合金(jin)化(hua)過程(cheng):在加熱(re)過程(cheng)中(zhong)(zhong),樣品會逐漸(jian)融化(hua)并(bing)開始重組,形成更緊密的晶格結(jie)構。在某(mou)些情況下,元素也可以在此過程(cheng)中(zhong)(zhong)重新分(fen)布,從而形成新的合金(jin)物質。

  5.冷卻:當(dang)燒(shao)結完成后,關(guan)閉加熱系統,并(bing)將(jiang)燒(shao)結爐(lu)(lu)緩慢降溫到室溫。在這個(ge)過程中,請(qing)不(bu)要(yao)打開爐(lu)(lu)門,以免樣品受到突(tu)然變化(hua)的影響。

  6.取(qu)出樣品(pin):當燒結爐完(wan)全冷卻之后,打開爐門,取(qu)出樣品(pin)托盤并檢(jian)查(cha)其質量。

  需要注意的(de)是(shi),不(bu)同的(de)燒(shao)結材(cai)料和(he)工藝流程可能(neng)會有所不(bu)同,因此在(zai)操作前請仔細閱讀設備和(he)材(cai)料的(de)使用說明書。

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立式真空速凝爐由哪些部分組成

立式真空速凝爐由哪些部分組成

  立式真空(kong)(kong)(kong)(kong)速凝(ning)爐(lu)(lu)(lu)由哪些部(bu)分(fen)(fen)組成(cheng)   立式真空(kong)(kong)(kong)(kong)速凝(ning)爐(lu)(lu)(lu)包括爐(lu)(lu)(lu)體(ti)(ti)、爐(lu)(lu)(lu)蓋(gai)、保溫桶(tong)、反射桶(tong)、發熱(re)(re)體(ti)(ti)、上(shang)(shang)(shang)壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)、下(xia)(xia)(xia)(xia)壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)、上(shang)(shang)(shang)油(you)缸、下(xia)(xia)(xia)(xia)油(you)缸和(he)抽真空(kong)(kong)(kong)(kong)部(bu)分(fen)(fen)。   其次,真空(kong)(kong)(kong)(kong)速凝(ning)爐(lu)(lu)(lu)帶上(shang)(shang)(shang)、下(xia)(xia)(xia)(xia)油(you)缸的支(zhi)撐(cheng)(cheng)機構為由熱(re)(re)軋槽(cao)鋼(gang)制(zhi)造的雙(shuang)立柱(zhu)式結(jie)(jie)構,上(shang)(shang)(shang)油(you)缸和(he)下(xia)(xia)(xia)(xia)油(you)缸分(fen)(fen)別裝設(she)在(zai)支(zhi)撐(cheng)(cheng)體(ti)(ti)上(shang)(shang)(shang)端(duan)(duan)和(he)底(di)座(zuo)中部(bu)。上(shang)(shang)(shang)油(you)缸通與荷(he)重傳(chuan)(chuan)感(gan)器連(lian)接(jie)(jie)(jie)(jie),荷(he)重傳(chuan)(chuan)感(gan)器下(xia)(xia)(xia)(xia)端(duan)(duan)與水(shui)冷(leng)(leng)壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)連(lian)接(jie)(jie)(jie)(jie),水(shui)冷(leng)(leng)壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)下(xia)(xia)(xia)(xia)端(duan)(duan)與上(shang)(shang)(shang)石(shi)(shi)墨壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)連(lian)接(jie)(jie)(jie)(jie)。下(xia)(xia)(xia)(xia)油(you)缸與下(xia)(xia)(xia)(xia)水(shui)冷(leng)(leng)壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)連(lian)接(jie)(jie)(jie)(jie),下(xia)(xia)(xia)(xia)水(shui)冷(leng)(leng)壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)與下(xia)(xia)(xia)(xia)石(shi)(shi)墨壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)連(lian)接(jie)(jie)(jie)(jie)。   通過(guo)焊(han)接(jie)(jie)(jie)(jie)固定在(zai)支(zhi)撐(cheng)(cheng)架的橫梁上(shang)(shang)(shang)中部(bu)。立式真空(kong)(kong)(kong)(kong)速凝(ning)爐(lu)(lu)(lu)在(zai)加熱(re)(re)室底(di)面(mian)上(shang)(shang)(shang)設(she)有(you)模(mo)(mo)具(ju)支(zhi)撐(cheng)(cheng)體(ti)(ti),成(cheng)型模(mo)(mo)具(ju)設(she)置在(zai)模(mo)(mo)具(ju)支(zhi)撐(cheng)(cheng)體(ti)(ti)上(shang)(shang)(shang)。圓(yuan)筒形加熱(re)(re)室設(she)置在(zai)爐(lu)(lu)(lu)體(ti)(ti)內,由托(tuo)盤(pan)結(jie)(jie)構進行定位,在(zai)立式真空(kong)(kong)(kong)(kong)熱(re)(re)壓(ya)(ya)(ya)(ya)燒結(jie)(jie)爐(lu)(lu)(lu)爐(lu)(lu)(lu)體(ti)(ti)和(he)加熱(re)(re)室的上(shang)(shang)(shang)、下(xia)(xia)(xia)(xia)端(duan)(duan)面(mian)上(shang)(shang)(shang)對稱地(di)開設(she)有(you)壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)通孔,上(shang)(shang)(shang)、下(xia)(xia)(xia)(xia)頂桿分(fen)(fen)別穿過(guo)加熱(re)(re)室上(shang)(shang)(shang)的壓(ya)(ya)(ya)(ya)頭(tou)(tou)(tou)通孔。三組引(yin)電(dian)電(dian)極(ji)(ji)分(fen)(fen)別裝有(you)絕緣(yuan)套和(he)熱(re)(re)輻射擋環,擋板位于加熱(re)(re)室內。三個引(yin)電(dian)電(dian)極(ji)(ji)分(fen)(fen)別通過(guo)水(shui)冷(leng)(leng)電(dian)極(ji)(ji)與石(shi)(shi)墨電(dian)極(ji)(ji)加熱(re)(re)體(ti)(ti)連(lian)接(jie)(jie)(jie)(jie)。立式真空(kong)(kong)(kong)(kong)熱(re)(re)壓(ya)(ya)(ya)(ya)燒結(jie)(jie)爐(lu)(lu)(lu)采用爐(lu)(lu)(lu)體(ti)(ti)和(he)爐(lu)(lu)(lu)蓋(gai)分(fen)(fen)離設(she)計,二者用六個鉸鏈(lian)螺栓通過(guo)爐(lu)(lu)(lu)耳和(he)密(mi)封(feng)圈密(mi)封(feng)結(jie)(jie)合。